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Katayarna, and J. Tanaka, Bull. Chem. Soc. , 1980,53, 1263. V. F. Kalasinky and S. Pechsiri, J. , 1980,9, 120. A. B. Nease and C. J. Wurrey, J. , 1980,9, 107. M. Ceroni and U. , 1979, 3703. '12This method may prove useful for the determination of molecular weights of epoxides. -Ring-opening Reactions. e. (124; R = CD3), which indicates a mechanism proceeding via the dicyclopropylcarbinylintermediate (123; R = CH, or CD,). ' Gf) 0 , OH (125) o@ 0 HO (126) (127) The reactions of a number of steroidal A-ring epoxides with electrophiles have been reported.
1981, 17,435 (Chem. , 1981,94,208 079). G . Kresze and M. Roessert, Liebigs Ann. , 1981,58. Meier and H. Kolshorn, 2. , Teil. 8, 1980,35,1040. 192 016). 32 Heterocyclic Chemistry Preparation of Aziridines by Cyclization. g. '~~ H OH Me0,C C0,Me MeozcwcozMe C0,Me (228) --* v C 0 , M e H (229) Two routes to 9,lO-iminophenanthrene (230) have been described. The l ~ ~ method involves the conversion of (231) into its a,a-dichloroalkyl phenyl ketimine (232) followed by its reduction by LiAlH4 in ether.
A m . Chem. ,1981,103,1913. R. Todeschini and G. Favini, I. Mol. , 1980,64,47. R. Todeschini, D. Pitea, and G. Favini, J. Mol. , 1981,71, 279. M. Traetteberg, T. W. Sandnes, and P. Bakken, J, Mol. , 1980,67, 235. P. Politzer, K. C. Daiker, and V. M. Estes, Int. J. , Quantum Biol. , 1979, 6,47. 103 W. H. Rastetter and J. Adams, J. Org. , 1980,45, 3534. 18 Heterocyclic Chemistry H-bonding solvent DMSO, however, the coupling constant is reduced, as intermolecular H-bonding with solvent becomes more important, down to a minimum value in 100% DMSO.