By Leo A. Paquette
There are lots of books on hand in regards to the chemistry and biology of sulfur. although, this is often the 1st booklet with a compilation of all correct Sulfur containing reagents. man made chemists, such a lot relatively within the medicinal and pharmaceutical chemists, are usually known as upon to organize compounds that include Sulfur as a key structural function. some time past, this looked to be a website for experts; this present day each artificial chemist operating in those region is anticipated to synthesize compounds containing sulfides, sulfates, sulfones, and so forth. This ebook bargains a massive resource of knowledge for the choice and dealing with of the precise reagents.
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There are lots of books to be had in regards to the chemistry and biology of sulfur. despite the fact that, this can be the 1st publication with a compilation of all suitable Sulfur containing reagents. artificial chemists, so much rather within the medicinal and pharmaceutical chemists, are usually referred to as upon to organize compounds that include Sulfur as a key structural function.
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Extra resources for Handbook of Reagents for Organic Synthesis, Sulfur-Containing Reagents
Lett. 1986, 527. 9. Labadie, S. , J. Org. Chem. 1989, 54, 2496. 10. Tonnet, M. ; Hambly, A. , Aust. J. Chem. 1971, 24, 703. 11. , J. Chem. Soc. (B) 1968, 1294. Synthesis of Protected β-Amino Acids. 1 O Raj K. Raheja & Carl R. Johnson Wayne State University, Detroit, MI, USA S NH2 O a. PhCHO, TiCl4 61% or b. 5 ◦ C. Form Supplied in: yellow solid; synthetically available. 37 (‘d’, J = 9 Hz, 2H). 1 1. ClSO3H 2. 3 In this case, however, better results were obtained with the less desirable N-tosyl imine (eq 6).
The enantiomers are obtained through use of an appropriate chiral auxiliary. Bis-sulfoxide 1 has been applied to the desymmetrization of a poly-oxygenated meso-diol containing ﬁve stereogenic centers (eq 2). BnO Introduction. (1R,5R)-2H-1,5-Benzodithiepin-3(4H)-one 1,5-dioxide (C2 -symmetric bis-sulfoxide 1) has been used as a chiral auxiliary for asymmetric desymmetrization of cyclic meso-1,2-diols via diastereoselective acetal cleavage reaction. The procedure consists of three steps (eq 1), that is, acetalization (step 1), acetal cleavage reaction followed by benzylation (step 2), and hydrolysis of the vinyl ether (step 3).
J. Org. Chem. 1986, 51, 1882. 4. Muller, G. ; Walters, D. ; Du Bois, G. , J. Med. Chem. 1992, 35, 740. 5. Miller, A. ; Feeney, D. ; Aziz, M. , Synth. Commun. 1990, 20, 217. 6. Suryawanshi, S. ; Bhakuni, D. , Indian J. , Sect. B 1991, 30B, 1089. 7. , J. Chem. , Chem. Commun. 1990, 1216. 8. ; Gould, S. ; Hein, S. ; Keszler, D. , J. Org. Chem. 1987, 52, 2179. 9. Iwanowicz, E. ; Roberts, D. G. ; Michel, I. ; Seiler, S. , Bioorg. Med. Chem. Lett. 1992, 2, 1607. 10. , Angew. , Int. Ed. Engl. 1992, 31, 785.
Handbook of Reagents for Organic Synthesis, Sulfur-Containing Reagents by Leo A. Paquette