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An Introduction to Spectroscopic Methods for the - download pdf or read online

By F. Scheinmann

ISBN-10: 0080066623

ISBN-13: 9780080066622

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Extra info for An Introduction to Spectroscopic Methods for the Identification of Organic Compounds. Nuclear Magnetic Resonance and Infrared Spectroscopy

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Soc, 1966, 88, 4811. 30. F. SONDHEIMER, R. WOLOVSKY, and Y. AMIEL, / . Amer. Chem. Soc, 1962, 84, 274. 31. L. M. JACKMAN, F. SONDHEIMER, Y. AMIEL, D. A. BEN-EFRAIM, Y. GAONI, R. WOLOVSKY, and A. A. BOTHNER-BY, / . Amer. Chem. Soc, 1962, 84, 4307. 32. F. SONDHEIMER, Y. GAONI, L. M. JACKMAN, N. A. BAILEY, and R. MASON, / . Amer. Chem. Soc, 1962, 84, 4595. CORRELATION TABLES FOR NUCLEAR MAGNETIC RESONANCE SPECTRA P. W. Hickmott and O. Meth-Cohn Contents page TABLE 1 τ-Values of α-protons in substituée alkanes 60 TABLE 2 Deshielding of alkyl protons by ß-substituents 61 TABLE 3 Shielding constants for disubstituted méthylènes (Shoolery's rules) TABLE 4 Approximate τ-values for H attached to unsaturated and aromatic groups 62 TABLE 5 τ-Values for protons attached to double bonds 64 TABLE 6 Proton chemical shifts in monosubstituted benzenes (Relative to benzene, 2-73 t) 65 61 TABLE 7a Proton chemical shifts (τ) in para-disubstituted benzenes for H (Relative to benzene, 2-73 τ) 66 TABLE 7b Proton chemical shifts (τ) in meta-disubstituted benzenes (Relative to benzene, 2-73 τ) 66 TABLE 8 τ-Values of acidic protons (—OH, —NH, and —SH) 67 TABLE 9 Proton spin-coupling constants 67 TABLE 10 τ-Values of some pro tic solvents 70 Correlation of dihedral angle with coupling constant JHU> (graph) 70 59 60 SPECTROSCOPIC METHODS VOLUME 1 TABLE 1 τ-VALUES OF OC-PROTONS IN SUBSTITUTED ALKANES CH 3 -X X R'CH 2 -X* R'R'CH-X 8-50 —R 910 8-75 -CH\ 1 8-68 a 7-6, 7-3 8-30 8-05 6 7-0 O R R ► ^— — — etc (end-of-chain position) J —C=C 8-20 7-5 — ^— — etc.

M. JACKMAN, J. Chem. Soc, 1961, 859. 28. I. C. CALDER and F. SONDHEIMER, Chem. , 1966, 904. 29. J. A. POPLE and K. G. UNTCH, / . Amer. Chem. Soc, 1966, 88, 4811. 30. F. SONDHEIMER, R. WOLOVSKY, and Y. AMIEL, / . Amer. Chem. Soc, 1962, 84, 274. 31. L. M. JACKMAN, F. SONDHEIMER, Y. AMIEL, D. A. BEN-EFRAIM, Y. GAONI, R. WOLOVSKY, and A. A. BOTHNER-BY, / . Amer. Chem. Soc, 1962, 84, 4307. 32. F. SONDHEIMER, Y. GAONI, L. M. JACKMAN, N. A. BAILEY, and R. MASON, / . Amer. Chem. Soc, 1962, 84, 4595. CORRELATION TABLES FOR NUCLEAR MAGNETIC RESONANCE SPECTRA P.

TORTORELLA, G. LUCENTE, and A. ROMEO, Ann. Chim. (Italy), 1960, 50, 1198. 11. J. R. NUNN, / . Chem. , 1952, 313; P. K. FAURE and J. C. SMITH, / . Chem. Soc, 1956, 1818. 12. K. L. RINEHART, W. A. NILSSON, and H. A. WHALEY, / . Amer. Chem. Soc, 1958, 80, 503. 13. S. G. SMITH and S. WINSTEIN, Tetrahedron, 1958, 3, 317. 14. E. W. ABEL, R. P. BUSH, F. J. HOPTON, and C. R. JENKINS, Chem. , 1966, 58. 15. J. M. Cox, J. A. ELVIDGE, and D. E. H. JONES, / . Chem. Soc, 1964, 1423. 16. C. F. CALLIS, J. R. VAN WAZER, J.

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An Introduction to Spectroscopic Methods for the Identification of Organic Compounds. Nuclear Magnetic Resonance and Infrared Spectroscopy by F. Scheinmann


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